ColumnUltisil® Diol (4.6×250 mm,5 μm)
Mobile PhaseN-hexane:isopropanol:10% glacial acetic acid=240:300:30 (add 0.05 mL of
triethylamine to each 100 mL of mobile phase), add glacial acetic acid after
mixing to adjust pH to 5.2
DetectionELSD
Drift Tube Temperature: 90℃
Airflow: 3.5 bar
Temperature40℃
Flow Rate1.0 ml/min
Injection Volume20 μL

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