Sys solution and intermediate 3

ColumnWelch Ultisil® PFP(4.6×150mm,3μm)
Wavelength215 nm
Temperature40℃
Flow Rate1.0 mL/min
Injection Volume10 μL

Mobile Phase

Time (min)0.1% trichloroacetic acid (%)Methanol (%)
04555
204555
401090

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