|Mobile Phase||Ammonium acetate and sodium perchlorate solution: take 4.0g ammonium acetate and 7.0g sodium perchlorate, add 1300mL. Wahaha dissolves it, adjusts the pH to 2.2 with phosphoric acid, shakes well, and ultrasonically degass.|
Ammonium acetate sodium perchlorate solution/acetonitrile = 85/15
|Flow Rate||1.0 ml/min|
|Injection Volume||10 μL|
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